Organic Syntheses

Time 2021-11-09 20:05:08

Web Name: Organic Syntheses

WebSite: http://www.orgsyn.org

ID:226790

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Organic,Syntheses,

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Top Volume 98 (2021) Zoom Articles Display Toggle all articles expansion 1 Discussion Addendum for: Intra- and Intermolecular Kulinkovich Cyclopropanation Reactions of Carboxylic Esters with Olefins: Bicyclo[3.1.0]hexan-1-ol and trans-2-benzyl-1-methylcyclopropan-1-ol Jin Kun Cha Org. Synth. 2021, 98, 430 DOI: 10.15227/orgsyn.098.0430 Original Article: Org. Synth. 2003, 80, 111

2 Preparation of 6-(Triethylsilyl)cyclohex-1-en-1-yl Trifluoromethanesulfonate as a Precursor to 1,2-Cyclohexadiene Ryo Nakura, Kazuki Inoue, Mayu Itoh, Atsunori Mori, and Kentaro Okano Org. Synth. 2021, 98, 407 DOI: 10.15227/orgsyn.098.0407 Checked by: Zhixun Wang and Kevin Campos

3 Preparation of (Bis)Cationic Nitrogen-Ligated I(III) Reagents: Synthesis of [(pyridine)2IPh](OTf)2 and [(4-CF3-pyridine)2IPh](OTf)2 Bilal Hoblos and Sarah E. Wengryniuk Org. Synth. 2021, 98, 391 DOI: 10.15227/orgsyn.098.0391 Checked by: Jeffrey T. Kuethe and Kevin R. Campos

4 Synthesis and Acylation of 1,3-Thiazinane-2-thione Stuart C. D. Kennington, Oriol Galeote, Miguel Mellado-Hidalgo, Pedro Romea and Fèlix Urpí Org. Synth. 2021, 98, 374 DOI: 10.15227/orgsyn.098.0374 Checked by: Zhaobin Han and Kuiling Ding

5 C2 Amination of Pyridine with Primary Amines Mediated by Sodium Hydride in the Presence of Lithium Iodide Jia Hao Pang, Derek Yiren Ong, and Shunsuke Chiba Org. Synth. 2021, 98, 363 DOI: 10.15227/orgsyn.098.0363 Checked by: Simon Cooper and Sarah Reisman

6 Catalytic Diazoalkane-Carbonyl Homologation: Synthesis of 2,2-Diphenylcycloheptanone and Other Quaternary or Tertiary Arylalkanones and Spirocycles by Ring Expansion Jason S. Kingsbury, Victor L. Rendina, Jacob S. Burman, and Brittany A. Smolarski Org. Synth. 2021, 98, 343 DOI: 10.15227/orgsyn.098.0343 Checked by: Junichi Taguchi, Haruka Fujino, and Masayuki Inoue

7 Preparation of 1-Benzyl-7-methylene-1,5,6,7-tetrahydro-4H-benzo[d]imidazol-4-one Michael Morgen, Jasmin Lohbeck, and Aubry K. Miller Org. Synth. 2021, 98, 315 DOI: 10.15227/orgsyn.098.0315 Checked by: Nageswara Rao Kalikinidi, Venumadhav Janganati, Gopal Sirasani, and Chris Senanayake

8 Synthesis of tert-Alkyl Phosphines: Preparation of Di-(1-adamantyl)phosphonium Trifluoromethanesulfonate and Tri-(1-adamantyl)phosphine Thomas Barber and Liam T. Ball Org. Synth. 2021, 98, 289 DOI: 10.15227/orgsyn.098.0289 Checked by: Praveen Kumar Gajula, Leila Terrab, Srinivasarao Tenneti, Gopal Sirasani, and Chris Senanayake

9 Preparation of Hindered Aniline CyanH and Application in the Allyl-Ni-Catalyzed ,-Dehydrogenation of Carbonyls Alexandra K. Bodnar, Aneta Turlik, David Huang, Will Butcher, Joanna K. Lew, and Timothy R. Newhouse Org. Synth. 2021, 98, 263 DOI: 10.15227/orgsyn.098.0263 Checked by: Aoi Takeuchi, Hiroaki Itoh, and Masayuki Inoue

10 Synthesis of Tetraaryl-, Pentaaryl-, and Hexaaryl-1,4-dihydropyrrolo[3,2-b]pyrroles Maciej Krzeszewski, Mariusz Tasior, Marek Grzybowski, and Daniel T. Gryko Org. Synth. 2021, 98, 242 DOI: 10.15227/orgsyn.098.0242 Checked by: Shu Nakamura, Koichi Hagiwara, and Masayuki Inoue

11 Preparation of 1-Hydrosilatrane, and Its Use in the Highly Practical Synthesis of Secondary and Tertiary Amines from Aldehydes and Ketones via Direct Reductive Amination Fawwaz Azam and Marc J. Adler Org. Synth. 2021, 98, 227 DOI: 10.15227/orgsyn.098.0227 Checked by: Jin Su Ham and Richmond Sarpong

12 Enantioselective Michael-Proton Transfer-Lactamization for Pyroglutamic Acid Derivatives: Synthesis of Dimethyl-(S,E)-5-oxo-3-styryl-1-tosylpyrrolidine-2,2-dicarboxylate Christian M. Chaheine, Conner J. Song, Paul T. Gladen, and Daniel Romo Org. Synth. 2021, 98, 194 DOI: 10.15227/orgsyn.098.0194 Checked by: Matthew J. Genzink and Tehshik P. Yoon

13 Mild mono-Acylation of 4,5-Diiodoimidazole: Preparation of 1-(5-Iodo-1H-imidazole-4-yl)pent-4-en-1-one Michael Morgen, Jasmin Lohbeck, and Aubry K. Miller Org. Synth. 2021, 98, 171 DOI: 10.15227/orgsyn.098.0171 Checked by: Anji Chen, Hari P. R. Mangunuru, Nathaniel D. Kaetzel, Gopal Sirasani, and Chris Senanayake

14 Synthesis of the Isocyanide Building Block Asmic, anisylsulfanylmethylisocyanide Embarek Alwedi, Bilal Altundas, Allen Chao, Zachary L. Ziminsky, Maanasa Natrayan, and Fraser F. Fleming Org. Synth. 2021, 98, 147 DOI: 10.15227/orgsyn.098.0147 Checked by: Anthony J. Fernandes, Martina Drescher, and Nuno Maulide

15 Palladium-Catalyzed Hydrodefluorination of Fluoroarenes Joseph J. Gair, Ronald L. Grey, Simon Giroux, and Michael A. Brodney Org. Synth. 2021, 98, 131 DOI: 10.15227/orgsyn.098.0131 Checked by: Vincent Porte, Daniel Kaiser, and Nuno Maulide

16 Discussion Addendum for: Preparation of (S)-tert-ButylPyOx and Palladium-Catalyzed Asymmetric Conjugate Addition of Arylboronic Acids Stephen R. Sardini and Brian M. Stoltz Org. Synth. 2021, 98, 117 DOI: 10.15227/orgsyn.098.0117 Original Article: Org. Synth. 2015, 92, 247

17 Synthesis of a Phosphorous Sulfur Incorporating Reagent for the Enantioselective Synthesis of Thiophosphates Prantik Maity, Amitha S. Anandamurthy, Vijaykumar Shekarappa, Rajappa Vaidyanathan, Bin Zheng, Jason Zhu, Michael A Schmidt, Richard J. Fox, Kyle W. Knouse, Julien C. Vantourout, Phil S. Baran, and Martin D. Eastgate Org. Synth. 2021, 98, 97 DOI: 10.15227/orgsyn.098.0097 Checked by: lvaro Gutirrez-Bonet and Kevin Campos

18 Cu-catalyzed Allylic Perfluoroalkylation of Alkenes Using Perfluoro Acid Anhydrides: Preparation of N-(5,5,5-Trifluoro-2-penten-1-yl)phthalimide Yuma Aoki, Shintaro Kawamura, and Mikiko Sodeoka Org. Synth. 2021, 98, 84 DOI: 10.15227/orgsyn.098.0084 Checked by: Martina Drescher, Daniel Kaiser, and Nuno Maulide

19 Palladium-Catalyzed Acetylation of Arylbromides Milauni M. Mehta, Andrew V. Kelleghan, and Neil K. Garg Org. Synth. 2021, 98, 68 DOI: 10.15227/orgsyn.098.0068 Checked by: Martina Drescher, Daniel Kaiser, Nuno Maulide, Zach Ariki, Yuki Maekawa, and Cathleen Crudden

20 Reductive Deuteration of Ketones with Magnesium and D2O for the Synthesis of -Deutero-o-methyl-benzhydrol Nengbo Zhu, Wen-Ming Wan, and Hongli Bao Org. Synth. 2021, 98, 51 DOI: 10.15227/orgsyn.098.0051 Checked by: Yuuki Watanabe, Koichi Hagiwara, and Masayuki Inoue

21 Chiral Organoiodine-catalyzed Enantioselective Oxidative Dearomatization of Phenols Muhammet Uyanik, Shinichi Ishizaki, and Kazuaki Ishihara Org. Synth. 2021, 98, 28 DOI: 10.15227/orgsyn.098.0028 Checked by: Tao Wang and Kevin Campos

22 Synthesis of Chiral Organoiodine Catalyst for Enantioselective Oxidative Dearomatization Reactions: N,N'-(2S,2'S )-(2-Iodo-1,3-phenylene)bis(oxy)bis(propane-2,1-diyl)bis(2,4,6-trimethylbenzamide) Muhammet Uyanik, Shinichi Ishizaki and Kazuaki Ishihara Org. Synth. 2021, 98, 1 DOI: 10.15227/orgsyn.098.0001 Checked by: Cayetana Zarate and Kevin Campos


Zoom Articles Display Show all current volume Board of Editors

Rick L. Danheiser
Massachusetts Institute of Technology
Editor-in-Chief

Kevin R. Campos
Merck Research Laboratories

Pauline Chiu
University of Hong Kong

Cathleen M. Crudden
Queen's University

Neil K. Garg
University of California, Los Angeles

Masayuki Inoue
University of Tokyo

Nuno Maulide
University of Vienna

Cristina Nevado
University of Zurich

Sarah E. Reisman
California Institute of Technology

Richmond Sarpong
University of California, Berkeley

Dirk Trauner
New York University

Seble Wagaw
AbbVie

Tehshik P. Yoon
University of Wisconsin, Madison

Charles K. Zercher
University of New Hampshire
Associate Editor

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